Information card for entry 4304940

Structure parameters

• Formula: C54 H126 N18 O57 Sb4 V20
• Calculated formula: C54 H126 N18 O57 Sb4 V20
• Title of publication: [V16Sb4O42(H2O){VO(C6H14N2)2}4]: A Terminal Expansion to a Polyoxovanadate Archetype
• Authors of publication: Adam Wutkowski; Christian Näther; Paul Kögerler; Wolfgang Bensch
• Journal of publication: Inorganic Chemistry
• Year of publication: 2008
• Journal volume: 47
• Pages of publication: 1916 - 1918
• a: 13.6528 ± 0.0011 Å
• b: 21.0096 ± 0.0011 Å
• c: 22.8018 ± 0.0016 Å
• α: 90°
• β: 100.004 ± 0.009°
• γ: 90°
• Cell volume: 6441 ± 0.8 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.05
• Residual factor for significantly intense reflections: 0.039
• Weighted residual factors for significantly intense reflections: 0.1006
• Weighted residual factors for all reflections included in the refinement: 0.1058
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No