Information card for entry 4304953

Structure parameters

• Chemical name: Lithium tetrahydrofuran nonakis(tert-butoxide) Uranium(IV) dimer
• Formula: C45 H101 Li O10 U2
• Calculated formula: C45.006 H63 Li O10 U2
• Title of publication: Synthesis and Characterization of Three Homoleptic Alkoxides of Uranium: [Li(THF)]2[UIV(OtBu)6], [Li(Et2O)][UV(OtBu)6], and UVI(OtBu)6
• Authors of publication: Skye Fortier; Guang Wu; Trevor W. Hayton
• Journal of publication: Inorganic Chemistry
• Year of publication: 2008
• Journal volume: 47
• Pages of publication: 4752 - 4761
• a: 41.314 ± 0.004 Å
• b: 11.0644 ± 0.001 Å
• c: 12.6456 ± 0.0011 Å
• α: 90°
• β: 101.592 ± 0.002°
• γ: 90°
• Cell volume: 5662.6 ± 0.9 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 12
• Hermann-Mauguin space group symbol: C 1 2/m 1
• Hall space group symbol: -C 2y
• Residual factor for all reflections: 0.0837
• Residual factor for significantly intense reflections: 0.0565
• Weighted residual factors for significantly intense reflections: 0.1536
• Weighted residual factors for all reflections included in the refinement: 0.1674
• Goodness-of-fit parameter for all reflections included in the refinement: 1.046
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No