Information card for entry 4305303

Structure parameters

• Formula: C34 H44 F12 N6 Ni3 O12
• Calculated formula: C34 H44 F12 N6 Ni3 O12
• Title of publication: Extended Triple-Bridged Ni(II)- and Co(II)-Hydroxamate Trinuclear Complexes: Synthesis, Crystal Structures, and Magnetic Properties
• Authors of publication: Z. Tomkowicz; S. Ostrovsky; H. Müller-Bunz; A. J. Hussein Eltmimi; M. Rams; D. A. Brown; W. Haase
• Journal of publication: Inorganic Chemistry
• Year of publication: 2008
• Journal volume: 47
• Pages of publication: 6956 - 6963
• a: 12.34 ± 0.002 Å
• b: 30.197 ± 0.005 Å
• c: 12.986 ± 0.002 Å
• α: 90°
• β: 92.645 ± 0.003°
• γ: 90°
• Cell volume: 4833.8 ± 1.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0578
• Residual factor for significantly intense reflections: 0.0472
• Weighted residual factors for significantly intense reflections: 0.116
• Weighted residual factors for all reflections included in the refinement: 0.1232
• Goodness-of-fit parameter for all reflections included in the refinement: 1.051
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No