Information card for entry 4305321

Structure parameters

• Formula: C74.25 H44.5 Br Cl4.5 F20 P4 Pd Pt2 Tl
• Calculated formula: C74.25 H40 Br Cl4.5 F20 P4 Pd Pt2 Tl
• Title of publication: Halide Addition/Abstraction in Phosphido Derivatives: Isolation of the Thallium and Silver Intermediates
• Authors of publication: Juan Forniés; Consuelo Fortuño; Susana Ibáñez; Antonio Martín
• Journal of publication: Inorganic Chemistry
• Year of publication: 2008
• Journal volume: 47
• Pages of publication: 5978 - 5987
• a: 15.293 ± 0.002 Å
• b: 24.708 ± 0.004 Å
• c: 20.794 ± 0.003 Å
• α: 90°
• β: 90.277 ± 0.003°
• γ: 90°
• Cell volume: 7857 ± 2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 9
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0521
• Residual factor for significantly intense reflections: 0.0373
• Weighted residual factors for significantly intense reflections: 0.0898
• Weighted residual factors for all reflections included in the refinement: 0.0958
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No