Information card for entry 4305397

Structure parameters

• Chemical name: (K-crypt)3[Sn9-C(CH3)3].2py
• Formula: C68 H127 K3 N8 O18 Sn9
• Calculated formula: C68 H127 K3 N8 O18 Sn9
• Title of publication: Tin-Based Organo-Zintl Ions: Alkylation and Alkenylation of Sn94-
• Authors of publication: Donald J. Chapman; Slavi C. Sevov
• Journal of publication: Inorganic Chemistry
• Year of publication: 2008
• Journal volume: 47
• Pages of publication: 6009 - 6013
• a: 14.4259 ± 0.0003 Å
• b: 16.2725 ± 0.0004 Å
• c: 22.5593 ± 0.0005 Å
• α: 86.092 ± 0.001°
• β: 78.952 ± 0.001°
• γ: 65.114 ± 0.001°
• Cell volume: 4714.48 ± 0.19 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 1
• Hermann-Mauguin space group symbol: P 1
• Hall space group symbol: P 1
• Residual factor for all reflections: 0.0406
• Residual factor for significantly intense reflections: 0.0348
• Weighted residual factors for significantly intense reflections: 0.0878
• Weighted residual factors for all reflections included in the refinement: 0.091
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No