Information card for entry 4305483

Structure parameters

• Formula: C15 H75 Cu N5 Na3 O76 P2 W17
• Calculated formula: C15 H45 Cu N5 Na O65.5 P2 W17
• Title of publication: Extended Organic-Inorganic Hybrids Based on Dawson and Double-Dawson-Type Polyoxometalates
• Authors of publication: Zhiming Zhang; Yangguang Li; Yonghui Wang; Yanfei Qi; Enbo Wang
• Journal of publication: Inorganic Chemistry
• Year of publication: 2008
• Journal volume: 47
• Pages of publication: 7615 - 7622
• a: 12.856 ± 0.003 Å
• b: 15.712 ± 0.003 Å
• c: 22.73 ± 0.005 Å
• α: 84.01 ± 0.03°
• β: 89.52 ± 0.03°
• γ: 68.41 ± 0.03°
• Cell volume: 4243.6 ± 1.8 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.139
• Residual factor for significantly intense reflections: 0.0742
• Weighted residual factors for significantly intense reflections: 0.1484
• Weighted residual factors for all reflections included in the refinement: 0.176
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No