Crystallography Open Database

Information card for entry 4305931

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Coordinates	4305931.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C18 H70 Cs8 O94 Si2 Sn3 W18
Calculated formula	C16 H15 Cs8 O76 Si2 Sn3 W18
Title of publication	Phenyltin-Substituted 9-Tungstogermanate and Comparison with Its Tungstosilicate Analogue
Authors of publication	Santiago Reinoso; Michael H. Dickman; Antonia Praetorius; Luis Fernando Piedra-Garza; Ulrich Kortz
Journal of publication	Inorganic Chemistry
Year of publication	2008
Journal volume	47
Pages of publication	8798 - 8806
a	32.8032 ± 0.0006 Å
b	16.252 ± 0.0003 Å
c	20.9576 ± 0.0005 Å
α	90°
β	120.675 ± 0.001°
γ	90°
Cell volume	9609.5 ± 0.4 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	7
Space group number	12
Hermann-Mauguin space group symbol	C 1 2/m 1
Hall space group symbol	-C 2y
Residual factor for all reflections	0.0763
Residual factor for significantly intense reflections	0.0543
Weighted residual factors for significantly intense reflections	0.1527
Weighted residual factors for all reflections included in the refinement	0.1674
Goodness-of-fit parameter for all reflections included in the refinement	1.078
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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