Information card for entry 4305987

Structure parameters

• Common name: ONb(OC[Ad]Mes)3(OEt2)
• Formula: C67 H92.5 Nb O5.75
• Calculated formula: C67 H92.5 Nb O5.75
• Title of publication: Phosphaalkenes as Long-Lived Phosphorus Cluster Surface Functional Groups: Intramolecular P=C Addition to a Niobium-Supported P7 Cage
• Authors of publication: Brandi M. Cossairt; Christopher C. Cummins
• Journal of publication: Inorganic Chemistry
• Year of publication: 2008
• Journal volume: 47
• Pages of publication: 9363 - 9371
• a: 12.592 ± 0.003 Å
• b: 14.536 ± 0.003 Å
• c: 17.436 ± 0.004 Å
• α: 73.72 ± 0.004°
• β: 78.872 ± 0.004°
• γ: 80.224 ± 0.004°
• Cell volume: 2983.1 ± 1.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0934
• Residual factor for significantly intense reflections: 0.0594
• Weighted residual factors for significantly intense reflections: 0.1596
• Weighted residual factors for all reflections included in the refinement: 0.183
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No