Information card for entry 4306530

Structure parameters

• Formula: C24 H20 N4 O Os
• Calculated formula: C24 H20 N4 O Os
• Title of publication: Oxidative ortho-C-N Fusion of Aniline by OsO4. Isolation, Characterization of Oxo-Amido Osmium(VI) Complexes, and their Catalytic Activities for Oxidative C-C Bond Cleavage of Unsaturated Hydrocarbons
• Authors of publication: Subhas Samanta; Laksmikanta Adak; Ranjan Jana; Golam Mostafa; Heikki M. Tuononen; Brindaban C. Ranu; Sreebrata Goswami
• Journal of publication: Inorganic Chemistry
• Year of publication: 2008
• Journal volume: 47
• Pages of publication: 11062 - 11070
• a: 14.036 ± 0.002 Å
• b: 4.927 ± 0.0009 Å
• c: 14.698 ± 0.003 Å
• α: 90°
• β: 95.07 ± 0.003°
• γ: 90°
• Cell volume: 1012.5 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 13
• Hermann-Mauguin space group symbol: P 1 2/n 1
• Hall space group symbol: -P 2yac
• Residual factor for all reflections: 0.0449
• Residual factor for significantly intense reflections: 0.0393
• Weighted residual factors for significantly intense reflections: 0.0873
• Weighted residual factors for all reflections included in the refinement: 0.0893
• Goodness-of-fit parameter for all reflections included in the refinement: 1.144
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No