Information card for entry 4306564

Structure parameters

• Formula: C132 H138 Cu10 P6 S12 Sn7
• Calculated formula: C132 H138 Cu10 P6 S12 Sn6.99
• Title of publication: A Heterometallic, Heterovalent CuI/SnII/IV/S Cluster with an Unprecedented Cu4Sn Core and Stannacyclopentane Units
• Authors of publication: Hari Pada Nayek; Werner Massa; Stefanie Dehnen
• Journal of publication: Inorganic Chemistry
• Year of publication: 2008
• Journal volume: 47
• Pages of publication: 9146 - 9148
• a: 17.6227 ± 0.0005 Å
• b: 22.6814 ± 0.0004 Å
• c: 18.8353 ± 0.0005 Å
• α: 90°
• β: 115.099 ± 0.002°
• γ: 90°
• Cell volume: 6817.7 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0768
• Residual factor for significantly intense reflections: 0.0377
• Weighted residual factors for significantly intense reflections: 0.0672
• Weighted residual factors for all reflections included in the refinement: 0.0734
• Goodness-of-fit parameter for all reflections included in the refinement: 0.834
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No