Crystallography Open Database

Information card for entry 4306634

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Coordinates	4306634.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C149 H238 Bi4 Cl10 Li6 O30
Calculated formula	C132 H206 Bi4 Cl10 Li6 O26
Title of publication	Synthesis and Characterization of Bismuth(III) and Antimony(III) Calixarene Complexes
Authors of publication	Lihua Liu; Lev N. Zakharov; James A. Golen; Arnold L. Rheingold; Tracy A. Hanna
Journal of publication	Inorganic Chemistry
Year of publication	2008
Journal volume	47
Pages of publication	11143 - 11153
a	16.0081 ± 0.0009 Å
b	20.2527 ± 0.001 Å
c	28.0539 ± 0.0015 Å
α	77.041 ± 0.001°
β	77.5 ± 0.001°
γ	75.926 ± 0.001°
Cell volume	8470.5 ± 0.8 Å³
Cell temperature	213 ± 2 K
Ambient diffraction temperature	213 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0623
Residual factor for significantly intense reflections	0.0392
Weighted residual factors for significantly intense reflections	0.1001
Weighted residual factors for all reflections included in the refinement	0.1075
Goodness-of-fit parameter for all reflections included in the refinement	0.97
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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