Information card for entry 4306682

Structure parameters

• Chemical name: N-tris-(trimethylsilyl)silyl-N-(trimethylsilyl)aminodichlorophosphane
• Formula: C12 H36 Cl2 N P Si5
• Calculated formula: C12 H36 Cl2 N P Si5
• SMILES: ClP(Cl)N([Si]([Si](C)(C)C)([Si](C)(C)C)[Si](C)(C)C)[Si](C)(C)C
• Title of publication: GaCl3-Assisted Cyclization Reactions in Hypersilyl(trimethylsilyl)aminodichlorophosphine
• Authors of publication: Alexander Villinger; Andrea Westenkirchner; Ronald Wustrack; Axel Schulz
• Journal of publication: Inorganic Chemistry
• Year of publication: 2008
• Journal volume: 47
• Pages of publication: 9140 - 9142
• a: 9.18 ± 0.0018 Å
• b: 17.44 ± 0.003 Å
• c: 17.069 ± 0.005 Å
• α: 90°
• β: 113.45 ± 0.02°
• γ: 90°
• Cell volume: 2507 ± 1.1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0453
• Residual factor for significantly intense reflections: 0.0312
• Weighted residual factors for significantly intense reflections: 0.0806
• Weighted residual factors for all reflections included in the refinement: 0.0859
• Goodness-of-fit parameter for all reflections included in the refinement: 1.044
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No