Information card for entry 4306693

Structure parameters

• Chemical name: μ-(Pyridyl-1,2)-μ-Hydrido-bis(pyridino-tricarbonyltechnetium)
• Formula: C21 H15 N3 O6 Tc2
• Calculated formula: C21 H15 N3 O6 Tc2
• Title of publication: C-H Bond Activation of Coordinated Pyridine: Ortho-Pyridyl-Ditechnetiumhydridocarbonyl Metal Cyclus. Crystal Structure and Dynamic Behavior in Solution
• Authors of publication: Maaz Zuhayra; Ulf Lützen; Arne Lützen; Laszlo Papp; Eberhard Henze; Gernot Friedrichs; Franz Oberdorfer
• Journal of publication: Inorganic Chemistry
• Year of publication: 2008
• Journal volume: 47
• Pages of publication: 10177 - 10182
• a: 10.088 ± 0.001 Å
• b: 10.088 ± 0.001 Å
• c: 19.817 ± 0.006 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 1746.5 ± 0.6 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 K
• Number of distinct elements: 5
• Space group number: 154
• Hermann-Mauguin space group symbol: P 32 2 1
• Hall space group symbol: P 32 2"
• Residual factor for all reflections: 0.0323
• Residual factor for significantly intense reflections: 0.0259
• Weighted residual factors for all reflections: 0.0729
• Weighted residual factors for significantly intense reflections: 0.0663
• Goodness-of-fit parameter for all reflections: 1.051
• Goodness-of-fit parameter for significantly intense reflections: 1.068
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No