Information card for entry 4306703

Structure parameters

• Chemical name: N-(trifluoromethylsulfonatodimethylsilyl)-N-[bis-(2,4,6-trimethylphenyl)phenyl] amino-trifluoromethylsulfonatomethylarsane toluene solvate
• Formula: C36 H42 As F6 N O6 S2 Si
• Calculated formula: C36 H42 As F6 N O6 S2 Si
• Title of publication: Lewis-Acid-Assisted Methyl Exchange Reactions In Silylated Aminodichloroarsanes
• Authors of publication: Dirk Michalik; Axel Schulz; Alexander Villinger
• Journal of publication: Inorganic Chemistry
• Year of publication: 2008
• Journal volume: 47
• Pages of publication: 11798 - 11806
• a: 12.241 ± 0.002 Å
• b: 20.94 ± 0.004 Å
• c: 15.639 ± 0.003 Å
• α: 90°
• β: 99.51 ± 0.03°
• γ: 90°
• Cell volume: 3953.6 ± 1.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0588
• Residual factor for significantly intense reflections: 0.0405
• Weighted residual factors for significantly intense reflections: 0.1108
• Weighted residual factors for all reflections included in the refinement: 0.1189
• Goodness-of-fit parameter for all reflections included in the refinement: 1.065
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No