Information card for entry 4306899

Structure parameters

• Formula: C37 H33 B Cl F20 P4 W
• Calculated formula: C37 H33 B Cl F20 P4 W
• Title of publication: Synthesis and Characterization of Cationic Tungsten(V) Methylidynes
• Authors of publication: Edwin F. van der Eide; Warren E. Piers; Masood Parvez; Robert McDonald
• Journal of publication: Inorganic Chemistry
• Year of publication: 2007
• Journal volume: 46
• Pages of publication: 14 - 21
• a: 27.5938 ± 0.0018 Å
• b: 11.9743 ± 0.0008 Å
• c: 13.3408 ± 0.0009 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4408 ± 0.5 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 7
• Space group number: 29
• Hermann-Mauguin space group symbol: P c a 21
• Hall space group symbol: P 2c -2ac
• Residual factor for all reflections: 0.0304
• Residual factor for significantly intense reflections: 0.0243
• Weighted residual factors for significantly intense reflections: 0.0528
• Weighted residual factors for all reflections included in the refinement: 0.0548
• Goodness-of-fit parameter for all reflections included in the refinement: 1.007
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No