Information card for entry 4306934

Structure parameters

• Chemical name: bis(dodecanethiolato)palladium(II)
• Formula: C24 H50 Pd S2
• Calculated formula: C24 H50 Pd S2
• Title of publication: Synthesis and Characterization of a New Tiara Pd(II) Thiolate Complex, [Pd(SC12H25)2]6, and Its Solution-Phase Thermolysis to Prepare Nearly Monodisperse Palladium Sulfide Nanoparticles
• Authors of publication: Zhiqiang Yang; Alexander B. Smetana; Christopher M. Sorensen; Kenneth J. Klabunde
• Journal of publication: Inorganic Chemistry
• Year of publication: 2007
• Journal volume: 46
• Pages of publication: 2427 - 2431
• a: 13.2189 ± 0.0014 Å
• b: 18.2919 ± 0.0018 Å
• c: 19.1575 ± 0.0019 Å
• α: 66.529 ± 0.005°
• β: 70.892 ± 0.008°
• γ: 77.054 ± 0.007°
• Cell volume: 3991.4 ± 0.7 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1456
• Residual factor for significantly intense reflections: 0.0618
• Weighted residual factors for significantly intense reflections: 0.1342
• Weighted residual factors for all reflections included in the refinement: 0.1616
• Goodness-of-fit parameter for all reflections included in the refinement: 0.859
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No