Information card for entry 4306941

Structure parameters

• Chemical name: complex 2
• Formula: C32 H29 B2 F8 N9 Ru
• Calculated formula: C32 H29 B2 F7.92 N9 Ru
• Title of publication: Synthesis of Pd Complexes Combined with Photosensitizing of a Ruthenium(II) Polypyridyl Moiety through a Series of Substituted Bipyrimidine Bridges. Substituent Effect of the Bridging Ligand on the Photocatalytic Dimerization of α-Methylstyrene
• Authors of publication: Akiko Inagaki; Shinichi Yatsuda; Shinichi Edure; Akiko Suzuki; Takeshi Takahashi; Munetaka Akita
• Journal of publication: Inorganic Chemistry
• Year of publication: 2007
• Journal volume: 46
• Pages of publication: 2432 - 2445
• a: 11.0233 ± 0.0015 Å
• b: 12.527 ± 0.003 Å
• c: 13.66 ± 0.003 Å
• α: 108.132 ± 0.005°
• β: 100.31 ± 0.009°
• γ: 98.311 ± 0.011°
• Cell volume: 1722.8 ± 0.6 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0837
• Residual factor for significantly intense reflections: 0.0552
• Weighted residual factors for significantly intense reflections: 0.1337
• Weighted residual factors for all reflections included in the refinement: 0.1504
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No