Information card for entry 4306943

Structure parameters

• Chemical name: complex4
• Formula: C33 H32 F12 N8 O P2 Ru
• Calculated formula: C33 H26 F11.94 N8 O P2 Ru
• Title of publication: Synthesis of Pd Complexes Combined with Photosensitizing of a Ruthenium(II) Polypyridyl Moiety through a Series of Substituted Bipyrimidine Bridges. Substituent Effect of the Bridging Ligand on the Photocatalytic Dimerization of α-Methylstyrene
• Authors of publication: Akiko Inagaki; Shinichi Yatsuda; Shinichi Edure; Akiko Suzuki; Takeshi Takahashi; Munetaka Akita
• Journal of publication: Inorganic Chemistry
• Year of publication: 2007
• Journal volume: 46
• Pages of publication: 2432 - 2445
• a: 13.247 ± 0.003 Å
• b: 23.613 ± 0.006 Å
• c: 12.127 ± 0.003 Å
• α: 90°
• β: 99.452 ± 0.018°
• γ: 90°
• Cell volume: 3741.8 ± 1.6 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/a 1
• Hall space group symbol: -P 2yab
• Residual factor for all reflections: 0.0677
• Residual factor for significantly intense reflections: 0.0511
• Weighted residual factors for significantly intense reflections: 0.1392
• Weighted residual factors for all reflections included in the refinement: 0.1499
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No