Information card for entry 4306977

Structure parameters

• Formula: C68 H72 Cl2 N4 O4 Pd4 S
• Calculated formula: C68 H72 Cl2 N4 O4 Pd4 S
• Title of publication: Genuine Examples of Tetrahedral Tetradentate Sulfide Ligand Bridging Four Pd Atoms: Controlled Formation of [(μ4-S){(μ2-X)Pd2(C^N)2}2] (X = OH or Cl; HC^N =p-C2H5OC6H4CHNC6H4-p-C2H5) Complexes
• Authors of publication: Rut Benavente; Pablo Espinet; José M. Martín-Álvarez; Jesús A. Miguel; Gabriel Aullón
• Journal of publication: Inorganic Chemistry
• Year of publication: 2007
• Journal volume: 46
• Pages of publication: 2035 - 2040
• a: 18.395 ± 0.004 Å
• b: 16.08 ± 0.003 Å
• c: 22.437 ± 0.005 Å
• α: 90°
• β: 104.752 ± 0.005°
• γ: 90°
• Cell volume: 6418 ± 2 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0843
• Residual factor for significantly intense reflections: 0.0382
• Weighted residual factors for significantly intense reflections: 0.0927
• Weighted residual factors for all reflections included in the refinement: 0.1294
• Goodness-of-fit parameter for all reflections included in the refinement: 1.003
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No