Information card for entry 4307054

Structure parameters

• Formula: C24 H50.66 K2 O74.33 S28 Th2 W12
• Calculated formula: C24 K2 O74.34 S28 Th2 W12
• Title of publication: Triangular Oxalate Clusters [W3(μ3-S)(μ2-S2)3(C2O4)3]2- as Building Blocks for Coordination Polymers and Nanosized Complexes
• Authors of publication: Maxim N. Sokolov; Artem L. Gushchin; Konstantin A. Kovalenko; Eugenia V. Peresypkina; Alexander V. Virovets; Joaquin Sanchiz; Vladimir P. Fedin
• Journal of publication: Inorganic Chemistry
• Year of publication: 2007
• Journal volume: 46
• Pages of publication: 2115 - 2123
• a: 14.1102 ± 0.0007 Å
• b: 14.2403 ± 0.0006 Å
• c: 14.8756 ± 0.0012 Å
• α: 106.73 ± 0.003°
• β: 102.71 ± 0.003°
• γ: 109.409 ± 0.002°
• Cell volume: 2529.6 ± 0.3 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0988
• Residual factor for significantly intense reflections: 0.0469
• Weighted residual factors for significantly intense reflections: 0.078
• Weighted residual factors for all reflections included in the refinement: 0.0943
• Goodness-of-fit parameter for all reflections included in the refinement: 1
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No