Information card for entry 4307060

Structure parameters

• Chemical name: catena-(tetrakis(μ~3~-Tropolonato-O,O,O',O')-(μ~3~-perchlorato-O,O',O'',O''') (μ~2~-perchlorato-O,O',O'',O''')-tri-lead(II))
• Formula: C14 H10 Cl O8 Pb1.5
• Calculated formula: C14 H10 Cl O8 Pb1.5
• Title of publication: Influence of pH and Counteranion on the Structure of Tropolonato-Lead(II) Complexes: Structural and Infrared Characterization of Formed Lead Compounds
• Authors of publication: Krzysztof Lyczko; Wojciech Starosta; Ingmar Persson
• Journal of publication: Inorganic Chemistry
• Year of publication: 2007
• Journal volume: 46
• Pages of publication: 4402 - 4410
• a: 12.03 ± 0.002 Å
• b: 9.0607 ± 0.0018 Å
• c: 14.652 ± 0.003 Å
• α: 90°
• β: 101.72 ± 0.03°
• γ: 90°
• Cell volume: 1563.8 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 13
• Hermann-Mauguin space group symbol: P 1 2/n 1
• Hall space group symbol: -P 2yac
• Residual factor for all reflections: 0.1039
• Residual factor for significantly intense reflections: 0.0474
• Weighted residual factors for significantly intense reflections: 0.1252
• Weighted residual factors for all reflections included in the refinement: 0.1565
• Goodness-of-fit parameter for all reflections included in the refinement: 1.009
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No