Information card for entry 4307140

Structure parameters

• Formula: C74 H152 K4 N10 Ni5 O24 Sb17
• Calculated formula: C74 H152.02 K4 N10 Ni5 O24 Sb17
• Title of publication: [Ni5Sb17]4-Transition-Metal Zintl Ion Complex: Crossing the Zintl Border in Molecular Intermetalloid Clusters
• Authors of publication: Melanie J. Moses; James C. Fettinger; Bryan W. Eichhorn
• Journal of publication: Inorganic Chemistry
• Year of publication: 2007
• Journal volume: 46
• Pages of publication: 1036 - 1038
• a: 15.51 ± 0.003 Å
• b: 16.661 ± 0.003 Å
• c: 25.943 ± 0.005 Å
• α: 86.253 ± 0.004°
• β: 81.86 ± 0.004°
• γ: 66.513 ± 0.003°
• Cell volume: 6086 ± 2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0768
• Residual factor for significantly intense reflections: 0.0443
• Weighted residual factors for significantly intense reflections: 0.1072
• Weighted residual factors for all reflections included in the refinement: 0.1168
• Goodness-of-fit parameter for all reflections included in the refinement: 1.074
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No