Information card for entry 4307198

Structure parameters

• Formula: H46 K10.5 O101 Si2 W22 Yb
• Calculated formula: K10.5 O101 Si2 W22 Yb
• Title of publication: The Monolanthanide-Containing Silicotungstates [Ln(β2-SiW11O39)2]13- (Ln = La, Ce, Sm, Eu, Gd, Tb, Yb, Lu): A Synthetic and Structural Investigation
• Authors of publication: Bassem S. Bassil; Michael H. Dickman; Bernd von der Kammer; Ulrich Kortz
• Journal of publication: Inorganic Chemistry
• Year of publication: 2007
• Journal volume: 46
• Pages of publication: 2452 - 2458
• a: 21.3738 ± 0.0005 Å
• b: 38.3275 ± 0.001 Å
• c: 25.3172 ± 0.0007 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 20740 ± 0.9 ų
• Cell temperature: 163 ± 2 K
• Ambient diffraction temperature: 163 ± 2 K
• Number of distinct elements: 6
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0962
• Residual factor for significantly intense reflections: 0.0639
• Weighted residual factors for significantly intense reflections: 0.1531
• Weighted residual factors for all reflections included in the refinement: 0.1745
• Goodness-of-fit parameter for all reflections included in the refinement: 1.005
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No