Information card for entry 4307368

Structure parameters

• Formula: C65 H153 I Mo6 N4 O27
• Calculated formula: C65 H144 I Mo6 N4 O27
• Title of publication: Protonation and Methylation of an Anderson-Type Polyoxoanion [IMo6O24]5-
• Authors of publication: Daisuke Honda; Shusaku Ikegami; Tomoaki Inoue; Tomoji Ozeki; Atsushi Yagasaki
• Journal of publication: Inorganic Chemistry
• Year of publication: 2007
• Journal volume: 46
• Pages of publication: 1464 - 1470
• a: 17.0679 ± 0.0004 Å
• b: 25.6998 ± 0.0006 Å
• c: 20.7428 ± 0.0004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 9098.7 ± 0.3 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 6
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0683
• Residual factor for significantly intense reflections: 0.041
• Weighted residual factors for significantly intense reflections: 0.1074
• Weighted residual factors for all reflections included in the refinement: 0.1278
• Goodness-of-fit parameter for all reflections included in the refinement: 1.016
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No