Information card for entry 4307415

Structure parameters

• Chemical name: Tetrakis(N,N-dimethylformamide)bis(μ~3~-oxo) hexakis(μ~2~-trifluoroacetate)bis(O-acetate)tetrairon(iii)
• Formula: C28 H28 F24 Fe4 N4 O22
• Calculated formula: C28 H28 F24 Fe4 N4 O22
• Title of publication: Synthesis and Reactivity of Haloacetato Derivatives of Iron(II) Including the Crystal and the Molecular Structure of [Fe(CF3COOH)2(μ-CF3COO)2]n
• Authors of publication: Fabio Marchetti; Fabio Marchetti; Bernardo Melai; Guido Pampaloni; Stefano Zacchini
• Journal of publication: Inorganic Chemistry
• Year of publication: 2007
• Journal volume: 46
• Pages of publication: 3378 - 3384
• a: 16.09 ± 0.001 Å
• b: 16.09 ± 0.001 Å
• c: 48.867 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 12651.1 ± 1.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 122
• Hermann-Mauguin space group symbol: I -4 2 d
• Hall space group symbol: I -4 2bw
• Residual factor for all reflections: 0.0668
• Residual factor for significantly intense reflections: 0.0617
• Weighted residual factors for significantly intense reflections: 0.158
• Weighted residual factors for all reflections included in the refinement: 0.1644
• Goodness-of-fit parameter for all reflections included in the refinement: 1.067
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No