Crystallography Open Database

Information card for entry 4307428

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Coordinates	4307428.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C31 H42 La N5 Ni2 O22
Calculated formula	C31 H42 La N5 Ni2 O22
Title of publication	Series of Trinuclear NiIILnIIINiII Complexes Derived from 2,6-Di(acetoacetyl)pyridine: Synthesis, Structure, and Magnetism
Authors of publication	Takuya Shiga; Nobuhiro Ito; Akiko Hidaka; Hisashi Ōkawa; Susumu Kitagawa; Masaaki Ohba
Journal of publication	Inorganic Chemistry
Year of publication	2007
Journal volume	46
Pages of publication	3492 - 3501
a	7.87 ± 0.0004 Å
b	9.4406 ± 0.0004 Å
c	14.5086 ± 0.0005 Å
α	92.775 ± 0.002°
β	104.76 ± 0.002°
γ	91.309 ± 0.003°
Cell volume	1040.47 ± 0.08 Å³
Cell temperature	183.2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for significantly intense reflections	0.0281
Weighted residual factors for all reflections included in the refinement	0.0969
Goodness-of-fit parameter for all reflections included in the refinement	1
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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