Crystallography Open Database

Information card for entry 4307430

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Coordinates	4307430.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C31 H43 N5 Ni2 O22 Pr
Calculated formula	C31 H43 N5 Ni2 O22 Pr
Title of publication	Series of Trinuclear NiIILnIIINiII Complexes Derived from 2,6-Di(acetoacetyl)pyridine: Synthesis, Structure, and Magnetism
Authors of publication	Takuya Shiga; Nobuhiro Ito; Akiko Hidaka; Hisashi Ōkawa; Susumu Kitagawa; Masaaki Ohba
Journal of publication	Inorganic Chemistry
Year of publication	2007
Journal volume	46
Pages of publication	3492 - 3501
a	7.8083 ± 0.0007 Å
b	9.3987 ± 0.0006 Å
c	14.481 ± 0.001 Å
α	92.794 ± 0.002°
β	104.708 ± 0.004°
γ	91.285 ± 0.003°
Cell volume	1026.02 ± 0.13 Å³
Cell temperature	183.2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for significantly intense reflections	0.0284
Weighted residual factors for all reflections included in the refinement	0.0869
Goodness-of-fit parameter for all reflections included in the refinement	1.001
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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