Crystallography Open Database

Information card for entry 4307439

Preview

Coordinates	4307439.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H38 Gd N5 Ni2 O21
Calculated formula	C30 H38 Gd N5 Ni2 O21
Title of publication	Series of Trinuclear NiIILnIIINiII Complexes Derived from 2,6-Di(acetoacetyl)pyridine: Synthesis, Structure, and Magnetism
Authors of publication	Takuya Shiga; Nobuhiro Ito; Akiko Hidaka; Hisashi Ōkawa; Susumu Kitagawa; Masaaki Ohba
Journal of publication	Inorganic Chemistry
Year of publication	2007
Journal volume	46
Pages of publication	3492 - 3501
a	14.103 ± 0.001 Å
b	17.2153 ± 0.0009 Å
c	16.3096 ± 0.0008 Å
α	90°
β	99.328 ± 0.003°
γ	90°
Cell volume	3907.4 ± 0.4 Å³
Cell temperature	183.2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for significantly intense reflections	0.0465
Weighted residual factors for all reflections included in the refinement	0.0659
Goodness-of-fit parameter for all reflections included in the refinement	0.996
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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