Crystallography Open Database

Information card for entry 4307478

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Coordinates	4307478.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C136 H146 Ce4 Mn10 N8 O63
Calculated formula	C120 H104 Ce4 Mn10 N2 O59
Title of publication	High-Nuclearity Ce/Mn and Th/Mn Cluster Chemistry: Preparation of Complexes with [Ce4Mn10O10(OMe)6]18+ and [Th6Mn10O22(OH)2]18+ Cores
Authors of publication	Abhudaya Mishra; Anastasios J. Tasiopoulos; Wolfgang Wernsdorfer; Khalil A. Abboud; George Christou
Journal of publication	Inorganic Chemistry
Year of publication	2007
Journal volume	46
Pages of publication	3105 - 3115
a	32.408 ± 0.002 Å
b	16.9687 ± 0.0011 Å
c	27.6545 ± 0.0017 Å
α	90°
β	95.942 ± 0.002°
γ	90°
Cell volume	15126.1 ± 1.6 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1572
Residual factor for significantly intense reflections	0.0805
Weighted residual factors for significantly intense reflections	0.1866
Weighted residual factors for all reflections included in the refinement	0.2168
Goodness-of-fit parameter for all reflections included in the refinement	0.973
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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