Information card for entry 4307667

Structure parameters

• Formula: C53 N15 O45 Pd2 W12
• Calculated formula: C53 N15 O45 Pd2 W12
• Title of publication: Syntheses and Characterizations of Palladium-Based Molecular Triangle/Square Compounds and Hybrid Composites with Polyoxometalates
• Authors of publication: Kazuhiro Uehara; Ko Kasai; Noritaka Mizuno
• Journal of publication: Inorganic Chemistry
• Year of publication: 2007
• Journal volume: 46
• Pages of publication: 2563 - 2570
• a: 11.5984 ± 0.0004 Å
• b: 20.4269 ± 0.0007 Å
• c: 21.098 ± 0.001 Å
• α: 90.908 ± 0.002°
• β: 103.321 ± 0.002°
• γ: 99.633 ± 0.002°
• Cell volume: 4787.7 ± 0.3 ų
• Cell temperature: 153 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.0709
• Weighted residual factors for all reflections included in the refinement: 0.2664
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No