Crystallography Open Database

Information card for entry 4307701

Preview

Coordinates	4307701.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C103.7 H136 Cl11.8 F12 Mo6 P4 Pd2 Ru2 S11
Calculated formula	C103.7 H105 Cl11.8 F12 Mo6 P4 Pd2 Ru2 S11
Title of publication	Synthesis and Reactivity of a Bis(disulfide)-Bridged RuMo3S4 Double-Cubane Cluster: A New Family of Nona- or Decanuclear Mixed-Metal Sulfide Clusters with Two RuMo3S4 Units
Authors of publication	Izuru Takei; Koji Kobayashi; Keita Dohki; Masanobu Hidai
Journal of publication	Inorganic Chemistry
Year of publication	2007
Journal volume	46
Pages of publication	1045 - 1047
a	18.241 ± 0.003 Å
b	18.61 ± 0.003 Å
c	22.053 ± 0.004 Å
α	72.338 ± 0.007°
β	87.748 ± 0.008°
γ	69.835 ± 0.006°
Cell volume	6678 ± 2 Å³
Cell temperature	293.1 K
Number of distinct elements	9
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for significantly intense reflections	0.067
Weighted residual factors for all reflections included in the refinement	0.202
Goodness-of-fit parameter for all reflections included in the refinement	1.027
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKa
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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