Information card for entry 4307833

Structure parameters

• Common name: Re2(hpp)4(CF3CO2)2,4CH2Cl2
• Formula: C34 H52 Cl4 F6 N12 O4 Re2
• Calculated formula: C34.002 H52.004 Cl4.004 F6 N12 O4 Re2
• Title of publication: Better Understanding of the Species with the Shortest Re26+ Bonds and Related Re27+ Species with Tetraguanidinate Paddlewheel Structures
• Authors of publication: F. Albert Cotton; Naresh S. Dalal; Penglin Huang; Sergey A. Ibragimov; Carlos A. Murillo; Paula M. B. Piccoli; Chris M. Ramsey; Arthur J. Schultz; Xiaoping Wang; Qinliang Zhao
• Journal of publication: Inorganic Chemistry
• Year of publication: 2007
• Journal volume: 46
• Pages of publication: 1718 - 1726
• a: 9.459 ± 0.003 Å
• b: 10.728 ± 0.004 Å
• c: 11.194 ± 0.004 Å
• α: 93.392 ± 0.006°
• β: 103.51 ± 0.005°
• γ: 95.5 ± 0.006°
• Cell volume: 1095.5 ± 0.7 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0223
• Residual factor for significantly intense reflections: 0.021
• Weighted residual factors for significantly intense reflections: 0.0528
• Weighted residual factors for all reflections included in the refinement: 0.0536
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No