Information card for entry 4307835

Structure parameters

• Common name: [Re2(hpp)4F](TFPB)2
• Formula: C92 H72 B2 F48.96 N12 Re2
• Calculated formula: C92 H72 B2 F48.96 N12 Re2
• Title of publication: Better Understanding of the Species with the Shortest Re26+ Bonds and Related Re27+ Species with Tetraguanidinate Paddlewheel Structures
• Authors of publication: F. Albert Cotton; Naresh S. Dalal; Penglin Huang; Sergey A. Ibragimov; Carlos A. Murillo; Paula M. B. Piccoli; Chris M. Ramsey; Arthur J. Schultz; Xiaoping Wang; Qinliang Zhao
• Journal of publication: Inorganic Chemistry
• Year of publication: 2007
• Journal volume: 46
• Pages of publication: 1718 - 1726
• a: 13.1621 ± 0.0006 Å
• b: 14.8033 ± 0.0007 Å
• c: 26.0223 ± 0.0012 Å
• α: 87.37 ± 0.001°
• β: 88.908 ± 0.001°
• γ: 76.862 ± 0.001°
• Cell volume: 4932.1 ± 0.4 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0568
• Residual factor for significantly intense reflections: 0.041
• Weighted residual factors for significantly intense reflections: 0.0919
• Weighted residual factors for all reflections included in the refinement: 0.1026
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No