Information card for entry 4307897

Structure parameters

• Formula: C20 H35 Cl4 N5 O4 S2 Ti2
• Calculated formula: C20 H35 Cl4 N5 O4 S2 Ti2
• Title of publication: Reaction of p-Toluenesulfonylamide and M(NMe2)4 (M = Ti, V): Generation of Electron-Deficient Imido Complexes of Early Transition Metals
• Authors of publication: Christian Lorber; Robert Choukroun; Laure Vendier
• Journal of publication: Inorganic Chemistry
• Year of publication: 2007
• Journal volume: 46
• Pages of publication: 3192 - 3202
• a: 22.6523 ± 0.0017 Å
• b: 11.4504 ± 0.0008 Å
• c: 15.3571 ± 0.0011 Å
• α: 90°
• β: 128.659 ± 0.005°
• γ: 90°
• Cell volume: 3110.5 ± 0.4 ų
• Cell temperature: 180 K
• Ambient diffraction temperature: 180 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0597
• Residual factor for significantly intense reflections: 0.0317
• Weighted residual factors for all reflections: 0.0455
• Weighted residual factors for significantly intense reflections: 0.038
• Weighted residual factors for all reflections included in the refinement: 0.038
• Goodness-of-fit parameter for all reflections included in the refinement: 1.0804
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No