Information card for entry 4308154

Structure parameters

• Formula: C30 H112 Cu10 N20 O74 Si2 W18
• Calculated formula: C30 H70 Cu10 N20 O74 Si2 W18
• Title of publication: Combination of Lacunary Polyoxometalates and High-Nuclear Transition Metal Clusters under Hydrothermal Conditions. 3. Structure and Characterization of [Cu(enMe)2]2{[Cu(enMe)2(H2O)]2[Cu6(enMe)2(B-a-SiW9O34)2]}.4H2O
• Authors of publication: Shou-Tian Zheng; Da-Qiang Yuan; Jie Zhang; Guo-Yu Yang
• Journal of publication: Inorganic Chemistry
• Year of publication: 2007
• Journal volume: 46
• Pages of publication: 4569 - 4574
• a: 12.5105 ± 0.0002 Å
• b: 14.371 ± 0.0002 Å
• c: 17.2687 ± 0.0002 Å
• α: 98.834 ± 0.001°
• β: 110.744 ± 0.001°
• γ: 104.711 ± 0.001°
• Cell volume: 2704.58 ± 0.07 ų
• Cell temperature: 273 ± 2 K
• Ambient diffraction temperature: 273 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0605
• Residual factor for significantly intense reflections: 0.0469
• Weighted residual factors for significantly intense reflections: 0.1131
• Weighted residual factors for all reflections included in the refinement: 0.125
• Goodness-of-fit parameter for all reflections included in the refinement: 1.064
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No