Information card for entry 4308181

Structure parameters

• Formula: C22 H39 Cl4 N8 O17.5 Zn
• Calculated formula: C22 H32.5 Cl4 N8 O17.5 Zn
• Title of publication: A New Branched Phenanthroline Derivative Ligand: Synthesis, Solution Chemistry, and Crystal Structures of Copper(II) and Zinc(II) Complexes
• Authors of publication: Gianluca Ambrosi; Mauro Formica; Vieri Fusi; Luca Giorgi; Annalisa Guerri; Mauro Micheloni; Paola Paoli; Roberto Pontellini; Patrizia Rossi
• Journal of publication: Inorganic Chemistry
• Year of publication: 2007
• Journal volume: 46
• Pages of publication: 4737 - 4748
• a: 10.225 ± 0.006 Å
• b: 15.88 ± 0.001 Å
• c: 24.179 ± 0.002 Å
• α: 102.033 ± 0.007°
• β: 100.026 ± 0.006°
• γ: 105.365 ± 0.007°
• Cell volume: 3591 ± 2 ų
• Cell temperature: 298 K
• Ambient diffraction temperature: 298 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.2131
• Residual factor for significantly intense reflections: 0.08
• Weighted residual factors for significantly intense reflections: 0.184
• Weighted residual factors for all reflections included in the refinement: 0.2263
• Goodness-of-fit parameter for all reflections included in the refinement: 0.849
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No