Information card for entry 4308293

Structure parameters

• Formula: C296 H253 Au18 Cl4 N3 O56 P16 V20
• Calculated formula: C296 H253 Au18 Cl4 N3 O56 P16 V20
• Title of publication: Structure-Directing Effects in the Supramolecular Intercluster Compound [Au9(PPh3)8]2[V10O28H3]2: Long-Range versus Short-Range Bonding Interactions
• Authors of publication: Martin Schulz-Dobrick; Martin Jansen
• Journal of publication: Inorganic Chemistry
• Year of publication: 2007
• Journal volume: 46
• Pages of publication: 4380 - 4382
• a: 22.51 ± 0.002 Å
• b: 33.749 ± 0.003 Å
• c: 46.872 ± 0.005 Å
• α: 90°
• β: 90.654 ± 0.002°
• γ: 90°
• Cell volume: 35606 ± 6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0652
• Residual factor for significantly intense reflections: 0.0444
• Weighted residual factors for significantly intense reflections: 0.1055
• Weighted residual factors for all reflections included in the refinement: 0.1138
• Goodness-of-fit parameter for all reflections included in the refinement: 0.993
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No