Information card for entry 4308381

Structure parameters

• Formula: C32 H68 N4 O8 Zn4
• Calculated formula: C32 H68 N4 O8 Zn4
• SMILES: [Zn]12([O]=C([O]3[Zn]4([O]=C([O]1[Zn]1([O]=C([O]2[Zn]3([O]=C([O]41)N(C(C)C)C(C)C)C)N(C(C)C)C(C)C)C)N(C(C)C)C(C)C)C)N(C(C)C)C(C)C)C
• Title of publication: Insertion Reactions of Carbon Dioxide into Zn‒N Bonds: Syntheses and Structures of Tetrameric and Dimeric Alkylzinc Carbamato Complexes
• Authors of publication: Tang, Yongjun; Kassel, W. Scott; Zakharov, Lev N.; Rheingold, Arnold L.; Kemp, Richard A.
• Journal of publication: Inorganic Chemistry
• Year of publication: 2005
• Journal volume: 44
• Journal issue: 2
• Pages of publication: 359 - 364
• a: 13.0143 ± 0.0004 Å
• b: 13.0143 ± 0.0004 Å
• c: 26.6298 ± 0.0016 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4510.3 ± 0.3 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 5
• Space group number: 76
• Hermann-Mauguin space group symbol: P 41
• Hall space group symbol: P 4w
• Residual factor for all reflections: 0.0292
• Residual factor for significantly intense reflections: 0.0262
• Weighted residual factors for significantly intense reflections: 0.0607
• Weighted residual factors for all reflections included in the refinement: 0.0617
• Goodness-of-fit parameter for all reflections included in the refinement: 0.997
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No