Information card for entry 4308383

Structure parameters

• Formula: C28 H52 N4 O8 Zn4
• Calculated formula: C28 H52 N4 O8 Zn4
• SMILES: C[Zn]12[O]3C(=[O][Zn]4(C)[O]5C(N6CCCCC6)=[O][Zn]3(C)[O](C(N3CCCCC3)=[O]2)[Zn]5(C)[O]=C(N2CCCCC2)[O]14)N1CCCCC1
• Title of publication: Insertion Reactions of Carbon Dioxide into Zn‒N Bonds: Syntheses and Structures of Tetrameric and Dimeric Alkylzinc Carbamato Complexes
• Authors of publication: Tang, Yongjun; Kassel, W. Scott; Zakharov, Lev N.; Rheingold, Arnold L.; Kemp, Richard A.
• Journal of publication: Inorganic Chemistry
• Year of publication: 2005
• Journal volume: 44
• Journal issue: 2
• Pages of publication: 359 - 364
• a: 14.3865 ± 0.0004 Å
• b: 14.3865 ± 0.0004 Å
• c: 8.8462 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1830.91 ± 0.13 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 5
• Space group number: 86
• Hermann-Mauguin space group symbol: P 42/n :2
• Hall space group symbol: -P 4bc
• Residual factor for all reflections: 0.0303
• Residual factor for significantly intense reflections: 0.0256
• Weighted residual factors for significantly intense reflections: 0.066
• Weighted residual factors for all reflections included in the refinement: 0.0685
• Goodness-of-fit parameter for all reflections included in the refinement: 1.007
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No