Information card for entry 4308426

Structure parameters

• Formula: C34.5 H43.5 N6 O4.75 Pb S2
• Calculated formula: C34.5 H43.5 N6 O4.75 Pb S2
• Title of publication: Novel Chiral "Calixsalen" Macrocycle and Chiral Robson-type Macrocyclic Complexes
• Authors of publication: Gao, Jian; Reibenspies, Joseph H.; Zingaro, Ralph A.; Woolley, F. Ross; Martell, Arthur E.; Clearfield, Abraham
• Journal of publication: Inorganic Chemistry
• Year of publication: 2005
• Journal volume: 44
• Journal issue: 2
• Pages of publication: 232 - 241
• a: 11.593 ± 0.003 Å
• b: 12.366 ± 0.003 Å
• c: 14.88 ± 0.004 Å
• α: 67.814 ± 0.004°
• β: 67.952 ± 0.004°
• γ: 88.071 ± 0.004°
• Cell volume: 1816.2 ± 0.8 ų
• Cell temperature: 110 ± 2 K
• Ambient diffraction temperature: 110 ± 2 K
• Number of distinct elements: 6
• Space group number: 1
• Hermann-Mauguin space group symbol: P 1
• Hall space group symbol: P 1
• Residual factor for all reflections: 0.0349
• Residual factor for significantly intense reflections: 0.0307
• Weighted residual factors for significantly intense reflections: 0.0751
• Weighted residual factors for all reflections included in the refinement: 0.0769
• Goodness-of-fit parameter for all reflections included in the refinement: 1.123
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No