Crystallography Open Database

Information card for entry 4308460

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Coordinates	4308460.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C36 H92 Cl2 N12 Ni6 O15
Calculated formula	C36 H2 Cl2 N12 Ni6 O15
Title of publication	Synthesis, Crystal Structure, and Magnetic Properties of Oxime-Bridged Polynuclear Ni(II) and Cu(II) Complexes
Authors of publication	Yun-Bo Jiang; Hui-Zhong Kou; Ru-Ji Wang; Ai-Li Cui; Joan Ribas
Journal of publication	Inorganic Chemistry
Year of publication	2005
Journal volume	44
Pages of publication	709 - 715
a	21.111 ± 0.001 Å
b	13.1963 ± 0.0008 Å
c	11.843 ± 0.0007 Å
α	90°
β	116.385 ± 0.001°
γ	90°
Cell volume	2955.6 ± 0.3 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	6
Space group number	12
Hermann-Mauguin space group symbol	C 1 2/m 1
Hall space group symbol	-C 2y
Residual factor for all reflections	0.0545
Residual factor for significantly intense reflections	0.0488
Weighted residual factors for significantly intense reflections	0.1317
Weighted residual factors for all reflections included in the refinement	0.1355
Goodness-of-fit parameter for all reflections included in the refinement	1.055
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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