Information card for entry 4308475

Structure parameters

• Formula: C32 H43 Cl2 N4 O6 V2
• Calculated formula: C16.5 H22.5 Cl2 N2 O3 V
• Title of publication: Family of Mixed-Valence Oxovanadium(IV/V) Dinuclear Entities Incorporating N4O3-Coordinating Heptadentate Ligands: Synthesis, Structure, and EPR Spectra
• Authors of publication: Amrita Mondal; Sumana Sarkar; Deepak Chopra; T. N. Guru Row; Kausikisankar Pramanik; Kajal Krishna Rajak
• Journal of publication: Inorganic Chemistry
• Year of publication: 2005
• Journal volume: 44
• Pages of publication: 703 - 708
• a: 18.461 ± 0.004 Å
• b: 17.23 ± 0.003 Å
• c: 13.7 ± 0.003 Å
• α: 90°
• β: 117.88 ± 0.03°
• γ: 90°
• Cell volume: 3851.9 ± 1.7 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1936
• Residual factor for significantly intense reflections: 0.102
• Weighted residual factors for all reflections: 0.3472
• Weighted residual factors for significantly intense reflections: 0.2568
• Goodness-of-fit parameter for all reflections: 0.958
• Goodness-of-fit parameter for significantly intense reflections: 1.114
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No