Information card for entry 4308483

Structure parameters

• Formula: C23 H52.6 Cl2 N6 Si2 Ti
• Calculated formula: C23 H52.6 Cl2 N6 Si2 Ti
• Title of publication: Synthesis of Titanium(IV) Guanidinate Complexes and the Formation of Titanium Carbonitride via Low-Pressure Chemical Vapor Deposition
• Authors of publication: Claire J. Carmalt; Anne C. Newport; Shane A. O'Neill; Ivan P. Parkin; Andrew J. P. White; David J. Williams
• Journal of publication: Inorganic Chemistry
• Year of publication: 2005
• Journal volume: 44
• Pages of publication: 615 - 619
• a: 8.9348 ± 0.0006 Å
• b: 13.1922 ± 0.0012 Å
• c: 13.9804 ± 0.0008 Å
• α: 90°
• β: 99.694 ± 0.005°
• γ: 90°
• Cell volume: 1624.3 ± 0.2 ų
• Cell temperature: 183 ± 2 K
• Ambient diffraction temperature: 183 ± 2 K
• Number of distinct elements: 6
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0408
• Residual factor for significantly intense reflections: 0.0367
• Weighted residual factors for significantly intense reflections: 0.0927
• Weighted residual factors for all reflections included in the refinement: 0.0948
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No