Information card for entry 4308510

Structure parameters

• Formula: C75 H134 Cl N17 Ni4 O9 S8
• Calculated formula: C75 H134 Cl N17 Ni4 O9 S8
• Title of publication: Structural Variety and Magnetic Properties of Tetranuclear Nickel(II) Complexes with a Central μ4-Azide
• Authors of publication: Serhiy Demeshko; Guido Leibeling; Walter Maringgele; Franc Meyer; Christopher Mennerich; Hans-Henning Klauss; Hans Pritzkow
• Journal of publication: Inorganic Chemistry
• Year of publication: 2005
• Journal volume: 44
• Pages of publication: 519 - 528
• a: 14.679 ± 0.002 Å
• b: 16.571 ± 0.002 Å
• c: 20.216 ± 0.003 Å
• α: 101.178 ± 0.003°
• β: 102.587 ± 0.003°
• γ: 90.957 ± 0.003°
• Cell volume: 4699.3 ± 1.1 ų
• Cell temperature: 297 ± 2 K
• Ambient diffraction temperature: 297 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0897
• Residual factor for significantly intense reflections: 0.0559
• Weighted residual factors for significantly intense reflections: 0.139
• Weighted residual factors for all reflections included in the refinement: 0.1671
• Goodness-of-fit parameter for all reflections included in the refinement: 1.077
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No