Crystallography Open Database

Information card for entry 4308550

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Coordinates	4308550.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C14 H21 I8 N7 U2
Calculated formula	C14 H21 I8 N7 U2
Title of publication	New Efficient Synthesis of [UI4(MeCN)4]. X-ray Crystal Structures of [UI2(MeCN)7][UI6], [UI4(py)3], and [U(dmf)9]I4
Authors of publication	Jean-Claude Berthet; Pierre Thuéry; Michel Ephritikhine
Journal of publication	Inorganic Chemistry
Year of publication	2005
Journal volume	44
Pages of publication	1142 - 1146
a	12.8779 ± 0.0009 Å
b	11.0818 ± 0.0011 Å
c	26.5236 ± 0.0015 Å
α	90°
β	90°
γ	90°
Cell volume	3785.2 ± 0.5 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	63
Hermann-Mauguin space group symbol	C m c m
Hall space group symbol	-C 2c 2
Residual factor for all reflections	0.0756
Residual factor for significantly intense reflections	0.0499
Weighted residual factors for significantly intense reflections	0.1078
Weighted residual factors for all reflections included in the refinement	0.1189
Goodness-of-fit parameter for all reflections included in the refinement	1.044
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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