Information card for entry 4308643

Structure parameters

• Common name: [Ni3salamo2(OAc)2(EtOH)2]
• Formula: C42 H52 N4 Ni3 O15
• Calculated formula: C42 H52 N4 Ni3 O15
• Title of publication: Novel Thiosalamo Ligand as a Remarkably Stable N2S2 Salen-Type Chelate and Synthesis of a Nickel(II) Complex
• Authors of publication: Shigehisa Akine; Tatsuya Nabeshima
• Journal of publication: Inorganic Chemistry
• Year of publication: 2005
• Journal volume: 44
• Pages of publication: 1205 - 1207
• a: 10.7606 ± 0.0017 Å
• b: 12.4817 ± 0.0018 Å
• c: 16.8606 ± 0.0019 Å
• α: 89.042 ± 0.006°
• β: 83.68 ± 0.006°
• γ: 78.832 ± 0.003°
• Cell volume: 2208.1 ± 0.5 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1005
• Residual factor for significantly intense reflections: 0.0551
• Weighted residual factors for significantly intense reflections: 0.1156
• Weighted residual factors for all reflections included in the refinement: 0.1335
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No