Information card for entry 4308668

Structure parameters

• Formula: C65.5 H52 Cl Ge5 Ir3 O5
• Calculated formula: C65.5 H52 Cl Ge5 Ir3 O5
• Title of publication: High-Nuclearity Iridium Carbonyl Clusters Containing Phenylgermyl Ligands: Synthesis, Structures, and Reactivity
• Authors of publication: Richard D. Adams; Burjor Captain; Jack L. Smith
• Journal of publication: Inorganic Chemistry
• Year of publication: 2005
• Journal volume: 44
• Pages of publication: 1413 - 1420
• a: 12.8208 ± 0.0008 Å
• b: 21.496 ± 0.0014 Å
• c: 23.5896 ± 0.0015 Å
• α: 90°
• β: 90.601 ± 0.001°
• γ: 90°
• Cell volume: 6500.8 ± 0.7 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0484
• Residual factor for significantly intense reflections: 0.0347
• Weighted residual factors for significantly intense reflections: 0.0961
• Weighted residual factors for all reflections included in the refinement: 0.1076
• Goodness-of-fit parameter for all reflections included in the refinement: 1.075
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No