Information card for entry 4308670

Structure parameters

• Formula: C64.5 H55 Cl Ge6 Ir4 O4
• Calculated formula: C64.5 H55 Cl Ge6 Ir4 O4
• Title of publication: High-Nuclearity Iridium Carbonyl Clusters Containing Phenylgermyl Ligands: Synthesis, Structures, and Reactivity
• Authors of publication: Richard D. Adams; Burjor Captain; Jack L. Smith
• Journal of publication: Inorganic Chemistry
• Year of publication: 2005
• Journal volume: 44
• Pages of publication: 1413 - 1420
• a: 23.6617 ± 0.001 Å
• b: 14.9749 ± 0.0006 Å
• c: 19.5807 ± 0.0008 Å
• α: 90°
• β: 103.784 ± 0.001°
• γ: 90°
• Cell volume: 6738.3 ± 0.5 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0391
• Residual factor for significantly intense reflections: 0.0296
• Weighted residual factors for significantly intense reflections: 0.0749
• Weighted residual factors for all reflections included in the refinement: 0.085
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No