Information card for entry 4308969

Structure parameters

• Formula: C138 H144 Ni3 O18 P6
• Calculated formula: C138.008 H144 Ni3 O18 P6
• Title of publication: 2-Phosphinophenolate Complexes: Formation and Crystal Structure of a Novel Trinuclear μ-O Nickel(II)-Tris(PO-Chelate)
• Authors of publication: Joachim Heinicke; Normen Peulecke; Konstantin Karaghiosoff; Peter Mayer
• Journal of publication: Inorganic Chemistry
• Year of publication: 2005
• Journal volume: 44
• Pages of publication: 2137 - 2139
• a: 15.344 ± 0.003 Å
• b: 21.235 ± 0.004 Å
• c: 19.134 ± 0.004 Å
• α: 90°
• β: 101.82 ± 0.03°
• γ: 90°
• Cell volume: 6102 ± 2 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1391
• Residual factor for significantly intense reflections: 0.0705
• Weighted residual factors for significantly intense reflections: 0.18
• Weighted residual factors for all reflections included in the refinement: 0.2145
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No