Information card for entry 4308999

Structure parameters

• Formula: C32 H35 Cl F6 N2 O3 P2 Re
• Calculated formula: C32 H35 Cl F6 N2 O3 P2 Re
• Title of publication: Reactivity of Rhenium(V) Oxo Schiff Base Complexes with Phosphine Ligands: Rearrangement and Reduction Reactions
• Authors of publication: Paul D. Benny; Jenny L. Green; Hendrik P. Engelbrecht; Charles L. Barnes; Silvia S. Jurisson
• Journal of publication: Inorganic Chemistry
• Year of publication: 2005
• Journal volume: 44
• Pages of publication: 2381 - 2390
• a: 10.3094 ± 0.001 Å
• b: 12.1196 ± 0.0012 Å
• c: 14.8146 ± 0.0015 Å
• α: 105.939 ± 0.002°
• β: 105.383 ± 0.002°
• γ: 93.525 ± 0.002°
• Cell volume: 1698 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0323
• Residual factor for significantly intense reflections: 0.0277
• Weighted residual factors for significantly intense reflections: 0.0701
• Weighted residual factors for all reflections included in the refinement: 0.0738
• Goodness-of-fit parameter for all reflections included in the refinement: 1.073
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No